Crystal Structure Analysis
Principles and Practice
Series: International Union of Crystallography Texts on Crystallography; 13;
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Product details:
- Edition number 2
- Publisher OUP Oxford
- Date of Publication 18 June 2009
- ISBN 9780199219469
- Binding Hardback
- No. of pages408 pages
- Size 252x198x24 mm
- Weight 1049 g
- Language English
- Illustrations 140 line drawings and halftones 0
Categories
Short description:
This text focuses on the practical aspects of crystal structure analysis and provides the necessary conceptual framework for understanding and applying the technique. Many worked examples, problems with answers, and illustrations are included throughout to reinforce the material presented. Significantly updated from the first edition.
MoreLong description:
This text focuses on the practical aspects of crystal structure analysis, and provides the necessary conceptual framework for understanding and applying the technique. By choosing an approach that does not put too much emphasis on the mathematics involved, the book gives practical advice on topics such as growing crystals, solving and refining structures, and understanding and using the results. The technique described is a core experimental method in modern structural chemistry, and plays an ever more important role in the careers of graduate students, postdoctoral and academic staff in chemistry, and final-year undergraduates.
Much of the material of the first edition has been significantly updated and expanded, and some new topics have been added. The approach to several of the topics has changed, reflecting the book's new authorship, and recent developments in the subject.
`Review from previous edition 'Graduate students, lecturers, and professionals in crystallography, solid state chemistry, condensed matter physics, structural biology, and materials science, will find the thrust of this book exciting ... Professionals in the field would be morally and professionally remiss if they failed to read, consult and discuss this volume with students and colleagues. Amongst several features contributing towards making the book an important acquisition are: comprehensive and up-to-date character; emphasis on practical aspects of the topic; inclusion of many worked examples and problems; and an abundance of illustrative material throughout.'
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Current Engineering Practice
Table of Contents:
Introduction to diffraction
Introduction to symmetry and diffraction
Crystal growth and evaluation
Space group determination
Background theory for data collection
Practical aspects of data collection
Practical aspects of data processing
Fourier syntheses
Patterson syntheses for structure determination
Direct methods of crystal structure determination
An introduction to maximum entropy
Least squares fitting of parameters
Refinement of crystal structures
Analysis of extended inorganic structures
The derivation of results
Random and systematic errors
Powder diffraction
Introduction to twinning
The presentation of results
The Crystallographic Information File (CIF)
Crystallographic databases
X-ray and neutron sources
Appendix A: Useful mathematics and formulae
Appendix B: Questions and answers
The Impact of Emerging Technologies on Reference Service and Bibliographic Instruction
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