Organocopper Reagents: A Practical Approach
A Practical Approach
Series: Practical Approach in Chemistry Series;
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Product details:
- Publisher OUP Oxford
- Date of Publication 30 March 1995
- ISBN 9780198557586
- Binding Paperback
- No. of pages376 pages
- Size 233x169x28 mm
- Weight 656 g
- Language English
- Illustrations line drawings, tables 0
Categories
Short description:
This essential laboratory handbook dispels the mystery surrounding organocopper compounds, and offers expert guidance on how to overcome the many problems associated with their use. Clear, practical procedures for the preparation and application of these highly specific reagents are described in detail by leading researchers.
MoreLong description:
BL Clear, experimental details in a convenient format
BL Practical advice from experienced researchers
BL Tried and tested methods
This new book launches the Practical Approach Series in Chemistry, especially for chemists who require practical and expert guidance on all aspects of chemical technique to achieve the best results - fast.
This essential laboratory handbook dispels the mystery surrounding organocopper compounds, and offers expert guidance on how to overcome the many problems associated with their use. Clear, practical procedures for the preparation and application of these highly specific reagents are described in detail by leading researchers.
Organocopper Reagents: A Practical Approach is a comprehensive laboratory guide which will prove invaluable to all organic chemists wishing to use copper reagents in synthesis. Both new and established researchers will find in this book all the information they need to enable them to exploit these powerful synthetic reagents to maximum effect.
It has been a pleasure to review this excellent volume. It will prove to be of value to academic and industrial practitioners of organic synthesis. I confidently expect that all reasearch laboratories will contain a copy. I hope that the publishers will be persuaded to standardise the drawings in future volumes - there are even differences within some chapters - so as to achieve a uniformity of presentation. Despite this minor criticism, all those connected with the production of this book are to be congratulated.
Table of Contents:
Organocopper chemistry: an overview
General procedures: starting materials and reaction guidelines
Preparation of reagents using activated copper
Preparation of highly functionalized reagents
Higher order cuprates
Me3SiCl accelerated conjugate additions
BF3/AlCl3 mediated conjugate addition and substitution reactions
Asymmetric conjugate addition
Conjugate addition - enolate trapping reactions
Sonogashira Cu/Pd catalysed alkyne coupling
Alkyne carbocupration and polyene synthesis via palladium catalysed coupling
Synthetic applications of silyl and stannyl cuprates
Mechanistic studies of organocopper reactions
Appendix 1: Compilation of organocopper preparations
Appendix 2: Suppliers of reagents and specialist items
Index
